氧氮氫分析儀的常見故障及解決方法:氧和氮空白值超過20。這是由于氣流小,,不能將爐子中的空氣驅(qū)趕出去,。可調(diào)節(jié)氣體流量,,調(diào)節(jié)載氣壓力在0.2~0.4MPa,。接通儀器載氣,放一個石墨坩堝在下電極上,,打開主電源開關(guān),,點擊軟件上的關(guān)爐按鈕,關(guān)閉爐子并等待10s,。調(diào)節(jié)流量調(diào)節(jié)器,,直到流量計a顯示為30L/h,打開爐子,。調(diào)節(jié)調(diào)節(jié)器直到流量計b顯示為50L/h,,再次關(guān)閉爐子。如果以上設(shè)置不穩(wěn)定,,則增加流量至100L/h,,反復調(diào)節(jié)直至儀器穩(wěn)定。上海禹重實業(yè)有限公司分析儀獲得眾多用戶的認可,。江蘇進口分析儀多少錢
Procedure-SolidSamplesDeterminetheinstrumentblank.Repeatsteps2bthrough2gaminimumofthreetimes.Settheblankfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.Instrumentcalibration/driftcorrection.Loginaminimumof3Standardreplicates.Weighapproximately***gramsofacalibration/driftstandard,enterthemassandstandardidentificationintoappropriatereplicatefields.Note:LECOReferenceMateria***onotrequirepreparation.Seepreparationstatementonthereferencematerialcertificate.山東美國分析儀哪家好上海禹重實業(yè)有限公司致力于提供分析儀,,竭誠為您服務,。
SamplePreparationSamplingandsamplepreparationofrefractorymetalssuchastitaniumandzirconiumissomewhatdifferentfromthatofsteel.Unlikesteelsamples,hydrogenisnotasmobileinthisgroupofmaterials;therefore,storageinliquidnitrogenordryiceisnotrequired.However,itisimportanttokeepthesamplecoolwhencuttingorsectioning.Samplepreparationforoxygenandnitrogendeterminationhasbeendifferentfromthatofhydrogendetermination.
SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.上海禹重實業(yè)有限公司為您提供分析儀,期待您的光臨,!
Procedure-SolidSamples:--Instrumentcalibration/driftcorrection.Placethenickelbasketcontainingthecalibration/driftstandardintotheopenportatthetopoftheloadinghead.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleaner.分析儀,,就選上海禹重實業(yè)有限公司,讓您滿意,,歡迎您的來電哦,!北京元素分析儀供應商
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氧氮氫分析儀的優(yōu)點采用惰氣熔融技術(shù),,同時測定氧、氮和氫元素含量新設(shè)計封閉氣路系統(tǒng),,優(yōu)化氣路循環(huán),,使氧氮氫測量更準確可采用更廉價的氬氣作為載氣催化爐溫度可調(diào),使氧的測量更加準確氣路系統(tǒng)都采用電磁閥控制,,新增分段式漏氣檢測水冷樣品加樣端口,,有效隔絕雜質(zhì)氣體侵入儀器配置和氧、氮,、氫測量范圍可靈活選擇新設(shè)計的高靈敏度紅外檢測池和熱導池,,有極低的檢出限分析時間短脈沖爐功率高達8.5kw,溫度3000℃顆粒狀樣品無需膠囊包裹,,使用經(jīng)濟實惠化學試劑及管路隱藏在門后(可移除)強大的分析軟件(支持數(shù)據(jù)和應用報告導出,、增加評論區(qū)及其他更多功能)。單點和多點校正(線性回歸)可采用自來水,、冷卻循環(huán)水機或交換機冷卻新設(shè)計的產(chǎn)品可用于各類生產(chǎn)控制和實驗室,。江蘇進口分析儀多少錢