氧氮?dú)浞治鰞x的優(yōu)點(diǎn)采用惰氣熔融技術(shù),同時(shí)測(cè)定氧,、氮和氫元素含量新設(shè)計(jì)封閉氣路系統(tǒng),,優(yōu)化氣路循環(huán),使氧氮?dú)錅y(cè)量更準(zhǔn)確可采用更廉價(jià)的氬氣作為載氣催化爐溫度可調(diào),,使氧的測(cè)量更加準(zhǔn)確氣路系統(tǒng)都采用電磁閥控制,,新增分段式漏氣檢測(cè)水冷樣品加樣端口,有效隔絕雜質(zhì)氣體侵入儀器配置和氧,、氮,、氫測(cè)量范圍可靈活選擇新設(shè)計(jì)的高靈敏度紅外檢測(cè)池和熱導(dǎo)池,有極低的檢出限分析時(shí)間短脈沖爐功率高達(dá)8.5kw,,溫度3000℃顆粒狀樣品無(wú)需膠囊包裹,,使用經(jīng)濟(jì)實(shí)惠化學(xué)試劑及管路隱藏在門(mén)后(可移除)強(qiáng)大的分析軟件(支持?jǐn)?shù)據(jù)和應(yīng)用報(bào)告導(dǎo)出、增加評(píng)論區(qū)及其他更多功能),。單點(diǎn)和多點(diǎn)校正(線性回歸)可采用自來(lái)水,、冷卻循環(huán)水機(jī)或交換機(jī)冷卻新設(shè)計(jì)的產(chǎn)品可用于各類生產(chǎn)控制和實(shí)驗(yàn)室。分析儀,,就選上海禹重實(shí)業(yè)有限公司,,讓您滿意,歡迎新老客戶來(lái)電,!專業(yè)分析儀
Procedure–Powder/ChipSamplesDeterminetheinstrumentblank.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically.Repeatsteps2bthrough2gaminimumofthreetimes.Settheblankfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.Instrumentcalibration/driftcorrection.LoginaminimumofthreeStandardreps.Weighapproximately***gramsofacalibration/driftstandardintoa***NickelCapsule;enterthemassandstandardidentificationintoappropriaterepfields.Ifapplicable,placethenickelcapsuleintheappropriateautoloaderposition.Note:LECOReferenceMateria***onotrequirepreparation.Seepreparationstatementonthereferencematerialcertificate.SolidStandardsmaybeusedtocalibratewhenchiporpowderstandardsarenotavailable.山東專業(yè)分析儀供應(yīng)商上海禹重實(shí)業(yè)有限公司為您提供分析儀,,歡迎您的來(lái)電哦!
Procedure-SolidSamplesPreparetheinstrumentasoutlinedintheoperatorsinstructionmanual.Determinetheinstrumentblank.Loginaminimumof3Blankreplicates.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Placea502-344NickelBasketintotheloadinghead.Note:samplesusingautomationshouldbeplacedintheappropriateautoloaderpositionbeforestartingtheanalysissequence.Oncethesequencehasstarted,theautomaticanalysiswillstartandendautomatically.
氧氮?dú)浞治鰞x的操作過(guò)程氧氮?dú)浞治鰞x可根據(jù)的用戶的要求定制,。該分析儀配備兩個(gè)不同靈敏度的探測(cè)器,,在更多的應(yīng)用中保證了準(zhǔn)確度。操作簡(jiǎn)單而且安全,。在樣品稱重以后,,樣品的重量數(shù)據(jù)通過(guò)電子界面?zhèn)鲗?dǎo)至相連的電腦中,也可以在軟件界面中手動(dòng)輸入樣品的重量,。樣品被放置在水平放置的爐子中的低溫區(qū)域,。分析開(kāi)始以后,爐子開(kāi)始向上轉(zhuǎn)動(dòng),,然后樣品逐漸落入加熱區(qū),。通過(guò)添加載體氣體氮?dú)猓瑲錃獗粩U(kuò)散出來(lái)并且隨載體被傳導(dǎo)至一個(gè)高靈敏度的熱傳導(dǎo)測(cè)量池。通常一次測(cè)量的時(shí)間在3到15分鐘之間,。在分析的過(guò)程中設(shè)備可以顯示測(cè)試信號(hào)和設(shè)備的參數(shù),,從信號(hào)的評(píng)估到結(jié)果在界面上的顯示全部自動(dòng)完成;而測(cè)量數(shù)據(jù)則被傳導(dǎo)至LIMS(實(shí)驗(yàn)室信息管理系統(tǒng))中,。無(wú)需過(guò)多的保養(yǎng)和維護(hù),,而除塵器和凈化管的維護(hù)工作也方便。上海禹重實(shí)業(yè)有限公司致力于提供分析儀,,有想法可以來(lái)我司咨詢,。
氧氮?dú)浞治鰞x的常見(jiàn)故障及解決方法:氧和氮空白值超過(guò)20。這是由于氣流小,,不能將爐子中的空氣驅(qū)趕出去,。可調(diào)節(jié)氣體流量,,調(diào)節(jié)載氣壓力在0.2~0.4MPa,。接通儀器載氣,放一個(gè)石墨坩堝在下電極上,,打開(kāi)主電源開(kāi)關(guān),,點(diǎn)擊軟件上的關(guān)爐按鈕,關(guān)閉爐子并等待10s,。調(diào)節(jié)流量調(diào)節(jié)器,,直到流量計(jì)a顯示為30L/h,打開(kāi)爐子,。調(diào)節(jié)調(diào)節(jié)器直到流量計(jì)b顯示為50L/h,,再次關(guān)閉爐子。如果以上設(shè)置不穩(wěn)定,,則增加流量至100L/h,,反復(fù)調(diào)節(jié)直至儀器穩(wěn)定。上海禹重實(shí)業(yè)有限公司致力于提供分析儀,,有想法的可以來(lái)電咨詢,!山東分析儀多少錢(qián)
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SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.專業(yè)分析儀